| Numéro |
J. Phys. IV France
Volume 7, Numéro C2, Avril 1997
Proceedings of the 9th International Conference on X-Ray Absorption Fine Structure
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|---|---|---|
| Page(s) | C2-1193 - C2-1194 | |
| DOI | https://doi.org/10.1051/jp4:19972189 | |
Proceedings of the 9th International Conference on X-Ray Absorption Fine Structure
J. Phys. IV France 7 (1997) C2-1193-C2-1194
DOI: 10.1051/jp4:19972189
1 Jozef Stefan Institute, Jamova 39, P.P. 3000, 1001 Ljubljana, Slovenia and Department of Physics, University of Ljubljana, Slovenia
2 Hamburger Synchrotronstrahlungslabor, DESY, Notkestrasse 85, 22603 Hamburg, Germany
© EDP Sciences 1997
J. Phys. IV France 7 (1997) C2-1193-C2-1194
DOI: 10.1051/jp4:19972189
EXAFS Study of Thermal Treatment of Pb-Zr Alkoxide Precursors
I. Arcon1, B. Malic1, A. Kodre1, M. Kosec1 and R. Frahm21 Jozef Stefan Institute, Jamova 39, P.P. 3000, 1001 Ljubljana, Slovenia and Department of Physics, University of Ljubljana, Slovenia
2 Hamburger Synchrotronstrahlungslabor, DESY, Notkestrasse 85, 22603 Hamburg, Germany
Abstract
The local environment of Zr atoms in amorphous precursors and intermediate products of the thermal treatment leading to perovskite PbZrO3 ceramic materials is studied by EXAFS. The coordination of Zr depends significantly on the choice of the starting Zr alkoxide. The Zr-O-Zr bond in an amorphous phase persists till the final stage of heating at 800 °C.
© EDP Sciences 1997